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By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by James P. BENNETT NETL – USDOE, USA

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Additional info for 12th INTERNATIONAL CERAMICS CONGRESS PART I Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART I including: Sym

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Both strength and specific fracture energy for crack initiation show a positive correlation with the percentage of transgranular crack propagation. Brittleness reduced materials therefore tend to show a lower amount of transgranular crack propagation resulting in a higher percentage of crack propagation along the grain/matrix interface. This finding is able to explain strength reduction. For the burnt and carbon bonded materials of this investigation magnesia grains (materials A-E) and corundum grains (material F) are the structure component with the highest density and strength.

Furthermore, dilatometry remains a method that allows identifying the temperature levels and ranges where microstructural changes take place. Fig. 3. Helpful test types to complete mechanical tests when studying monolithic castables: a) digital image correlation (DIC), b) in-situ high temperature environmental scanning microscopy (in-situ HTESEM), c) dilatometry. The different test types considered here (figures 2 and 3) have been described in details in previous papers [3,8,9,10,11]. 3. 1. Case of non-reinforced refractory monolithic castables For an andalusite based refractory concrete, examples of room temperature tensile test results are given in figure 4a.

A ∫0 (6) Here δult is the ultimate strain and A the projection of the fracture surface area. Moreover from the maximum horizontal load FH,max a nominal notch tensile strength can be calculated adding the tensile and the flexural component: σ NT = FH ,max  y 1 + 6  . b⋅h  h (7) In Eq. 7 b is the width and h the height of the specimen, and y denotes the vertical distance of the horizontal force from the center of gravity of the fracture surface. Approximate dimensions are 66 mm for h and 64 mm for b.

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12th INTERNATIONAL CERAMICS CONGRESS PART I Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART I including: Sym by Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by James P. BENNETT NETL – USDOE, USA


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